Fall 2015 - CHEM 316 D100

Introductory Instrumental Analysis (4)

Class Number: 3171

Delivery Method: In Person

Overview

  • Course Times + Location:

    Sep 8 – Dec 7, 2015: Tue, Fri, 12:30–1:20 p.m.
    Burnaby

  • Exam Times + Location:

    Dec 15, 2015
    Tue, 3:30–6:30 p.m.
    Burnaby

  • Prerequisites:

    CHEM 215 and CHEM 260, or permission of the department.

Description

CALENDAR DESCRIPTION:

Principles and applications of basic analytical instrumentation based upon spectroscopy, chromatography and electrochemistry. Students with credit for CHEM 416 may not take this course for further credit. Quantitative.

COURSE DETAILS:

2 lecture hours/week; a total of 4 labs in the semester

Clarification: Chem416 has not bee provided for more than 10 years, and will unlikely be provided in the future. Electrochemistry will not be focused in this course and has been covered by Chem215. The above mentioned description is a historical one and will be updated for spring 2016 semester.

This course will provide students basic knowledge and hands-on experience on a few widely used instruments in general applications. The theme is designed to help students develop skills in decision making, hypothesis testing, and critical thinking by exposing students to a variety of instrumental methodologies, working principles, and analysis design through well formulated lectures, in-class discussions, group projects, and labs.

Lecture Topics: 1. Instrument based compound characterization techniques --- atomic & molecular spectroscopic techniques (AAS, AES, ICPS, molecular absorption, molecular fluorescence; Beer's Law); 2. Instrument based separation techniques --- GC, LC, HPLC, SFC, CE, microfluidics, lab-on-a-chip, separation theory, van Deemter equation, detection systems, such as mass spectrometry (MS).

Laboratory Assignments: Labs include gas chromatography (GC), high performance liquid chromatography (HPLC), FID/MS, atomic absorption & emission spectroscopy (AAS & AES), molecular absorption & fluorescence spectroscopy.

COURSE-LEVEL EDUCATIONAL GOALS:

The course aims to build fundamental basics in students on using any instruments for analysis that occured not limited in chemistry, but also in physics, biology, material and environmental sciences; analysis occured not only in research, but also in applications of pharmaceutical industry, petroleum industry, criminology, as well as hospitals and clinics.

Grading

  • Midterm Exam 20%
  • Final Exam 40%
  • Laboratory 30%
  • Team Presentation 10%

NOTES:

The tuition for this course includes a fee of $7.50 for the laboratory manual.

REQUIREMENTS:

Students must pass BOTH the exam and laboratory portions to pass the course.

Materials

MATERIALS + SUPPLIES:

A hardbound lab notebook (not soft or coil bound)

REQUIRED READING:

Douglas A. Skoog, F. James Holler & Stanley R. Crouch. Principles of Instrumental Analysis: Custom Edition. 2014. Publisher: Brooks/Cole.

.or.

Douglas A. Skoog, F. James Holler & Stanley R. Crouch. Principles of Instrumental Analysis, 6th edition, Publisher: Brooks/Cole.

Lab manuals will be distributed during the first laboratory session.

Department Undergraduate Notes:

A grade of C- or better is required for all prerequisite courses.

Registrar Notes:

SFU’s Academic Integrity web site http://students.sfu.ca/academicintegrity.html is filled with information on what is meant by academic dishonesty, where you can find resources to help with your studies and the consequences of cheating.  Check out the site for more information and videos that help explain the issues in plain English.

Each student is responsible for his or her conduct as it affects the University community.  Academic dishonesty, in whatever form, is ultimately destructive of the values of the University. Furthermore, it is unfair and discouraging to the majority of students who pursue their studies honestly. Scholarly integrity is required of all members of the University. http://www.sfu.ca/policies/gazette/student/s10-01.html

ACADEMIC INTEGRITY: YOUR WORK, YOUR SUCCESS